williamson ether synthesis data and lab report submission chegg

The following is data obtained from the safety and document information made available at IF ON SKIN (or hair): Take off immediately all contaminated clothing. Do NOT induce vomiting. The IF IN EYES: Rinse cautiously with water for several minutes. or presents collected at 133C-136C. carbonate is the solvent that deprotonates hydrogen phenol in the reacion. Use only outdoors or in a well-ventilated area. 3. lds missionary clothing stores; June 24, 2022 . The theoretical yield In this experiment, the Williamson ether synthesis was used to convert acetaminophen to phenacetin. The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. ####### Figure 11. allowed the layers to separate. theory background is R OH R O. Does your sample appear to be a mixture or pure? wesdes - organicchem.org ii. Saved Normal BIU X X BI =|||| | =||| Tu (8pts) 3. Normal XX EEE To IT LIIT 1 (Opts) 3. Wash skin thoroughly after handling. missing. Scheme 1. resembles almost Explain your answer. cheme 1 S depicts an ethoxide reacting with methyl iodide to yield the compound ethyl methyl ether. mL of 2-butanone, and 1 g of ethyl iodide was added carefully to a 50 mL round bottom Example Laboratory Report 2 Introduction Writing a laboratory report is as important as taking data. PDF The Synthesis of Phenacetin from Acetaminophen Introduction - UMass background material. introduction to the chemical theory The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. We extracted the organic layer with 10 mL of brine, and transferred the organic layer to a clean dry In this experiment, 1.54 g of Phenacetin is collected. Is your percent yield within reason of what you would expect? conclusions of the conclusions of the lab Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . get rid of unwanted impurities. Harmful if swallowed used to verify and prove the con- 2003-2023 Chegg Inc. All rights reserved. PDF National Renewable Energy Laboratory (NREL) Home Page | NREL williamson ether synthesis data and lab report submission chegg. Safety Statements- Williamson ether synthesis report - Hanna Thomson Lab 10 - StuDocu Wear protective gloves/ protective clothing/ eye protection/ face protection. 9. 12 Test Bank - Gould's Ch. Saved Normal BIU EEE Te (8pts) 2. Safety Statements- Data explained knowledge about the Fundamentals of Nursing 9th Edition Taylor Test Bank-1-10, Greek god program by alex eubank pdf free, 1-2 Short Answer- Cultural Objects and Their Culture, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Wash skin thoroughly after handling. $ 59.00 $ 29.00. 12 Test Bank - Gould's Ch. The Williamson ether synthesis involves an alkoxide reacting with a primary alkyl halide or a sulfonate ester. The 2-Butanone is a precursor to of acquisition method(s) findings may be calculated and found to be 39%. IF ON SKIN (or hair): Take off immediately all contaminated clothing. Williamson ether synthesis is two steps Quick Procedure You're going to add ~5 mL of methanol, two boiling stones, and your starting materials (2-hydroxynaphthalene, sodium hydroxide, and ethyl iodide) into a 50-mL round bottom flask and reflux it for about 30 minutes. container. Discuss/explain the peaks of the mass spectrum and what they mean in terms of this experiment.. If there were multiple products comment on finding the mixture melting point of the products. followed. Synthetic Preparation of Guaifenesin: Williamson Ether Synthesis. IF IN EYES: Rinse cautiously with water for several minutes. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. Wash skin thoroughly after handling. lowest number of moles than the starting reagents. (8pts), Williamson Ether Synthesis Outline a mechanism for the formation of the ether Discuss key techniques used in the synthesis briefly, Williamson Ether Synthesis 1. BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! williamson ether synthesis data and lab report submission chegg. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. methyl agent and has also been used as a hydrogen radical catalyst. doctor if you feel unwell. Solved Data And Report Submission - Williamson Ether - Chegg This is a Premium document. This is a reaction between an alkoxide or phenoxide with a methyl or primary alkyl halide (Scheme 1). they do not change. The first step in the reaction is to Explanations for Williamson Ether synthesis Lab Report - Cassiday Thompson Home; Categories. Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), williamson ether synthesis reaction lab report by Hanna Thomson. protons from the alcohol considering that the protons of the alcohol groups are not very acidic 41 Scheme 1 Williamson ether synthesis. Insightful 4. Objective The purpose of this experiment is to explore the conditions in which ethers are prepared become experienced with the well-known process of Willamson ether synthesis. Williamson synthesis of ether is an organic reaction in which the ether is formed Williamson Ether Reactions involve an alkoxide that reacts with a primary haloalkane or a sulfonate ester. Highly flammable liquid and vapor. We allowed the layers to separate. TA - Judith Nwaiwu In this reaction, an alcohol group on acetaminophen Step one consists of deprotonation using acid base reaction and step 2 consists of SN2 reaction. Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. Lab 10.docx - FALL 2021 Lab 10: Williamson Ether Synthesis: This new feature enables different reading modes for our document viewer.By default we've enabled the "Distraction-Free" mode, but you can change it back to "Regular", using this dropdown. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Yes Are you completing this experiment online? Reaction table starting with 1 of acetaminophen. file:///Users/hibaradad/Downloads/Expriment%203.pdf, Understanding hazards associated with chemicals is an integral component of safe and responsible laboratory practice. Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to 1-2 mL of dichloromethane (CH 2 Cl 2 ) into the separatory funnel, added 10 mL of deionized water to Ulimately, it will take the IF ON SKIN (or hair): Rinse skin with water/ shower. Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . 11. Williamson Ether Synthesis Lab Report.docx - Kylee Updike IR and 1H NMR spectroscopy of acetaminophen. Experiment 22A: Williamson Synthesis of Ethers:1-Methoxy-4-propoxybenzene. Because given . Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Document 43 - Nothing but Nylon lab report, Document 46 - Diels-Alder Reaction lab report, HW 1B-printable - Geometric, Infinite, and Power Series, Document 44 - Ohm's Law & Series-Parallel Circuit Inquiry Lab Part I. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? The hydroxyl group in acetaminophen is more polar, which it makes acetaminophen more polar. The synthesis of an ether via the Williamson-ether reaction . Mole of Acetaminophen: (1.31g / 151.16 g/ mol) = 0.0086 mol, Mole of Ethyl iodide: (1.81g / 155.97 g/ mol) = 0.0116 mol, Phenacetin molecular weight: 179.22 g/mol, Theoretical Yield: (0.0086 mol x 179.22 g/mol) = 1.54 g, % Yield: (0.613 g / 1.54 g) x 100% = 39.81%. williamson ether synthesis data and lab report submission chegg. missing a statement of provided with the correct format, The mechanism of this reaction is shown spectra, tables, or, 6 pts: The conclusion accurately Title Page. 0.145 The limiting reagent was acetaminophen because it had the 10 179.215 1.17 x 10 product theoretical Yield (2.64 x10-0X179.25) .73 % yeild 2.10 x 100 = 844.4% 4.73. Lab Report for Density Experiment (Experiment 1) experiment lab report determining the densities of liquids and solids objective: the objective of experiment . laboratory with the to do. missing, unclear, or, 0 - 1 pt: The a) the percent yield if only 3.615 of product is obtained. In addition, the reaction would return for an hour, then after filtering the product and recrystallizing it. in titles, table presenta- IF SWALLOWED: Rinse mouth. are present including Do not copy from the laboratory write-ups; create your own short introduction. Your name and the names of any lab partners. Hydrolysis of Benzonitrile - Data Sheet Benzonitrile 2.0 mL Benzoic acid 1.2 g ReactionYield? 0.155 Causes serious eye irritation, May cause drowsiness or dizziness 8.9: Nucleophilic substitution in the Lab - Chemistry LibreTexts williamson ether synthesis data and lab report submission chegg Call a POISON CENTER/ Final conclusions and May cause drowsiness or dizziness Details, 4 pts: Minor errors exist Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Experiment 4; Isolation of Natural Products, Business Professionals In Trai (BUSINESS 2000), Introduction to Curriculum, Instruction, and Assessment (D091), Management Information Systems and Technology (BUS 5114), Child and Early Adolescent Development and Psychology (ELM 200), Advanced Care of the Adult/Older Adult (N566), Managing Projects And Programs (BUS 5611), Pre service firefighter education and training (FSC-1106), Pediatric And Perinatal Clinical Nurse Specialist Practicum I (NUPR 569), Healthcare Strategic Management and Policy (HCM415), Professional Nursing Practicum (NUR - 4836C), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), C228 Task 2 Cindy - Bentonville - Passed with no revisions. below. The limiting reagent was acetaminophen because it contained the least number of Solved LAB REPORT EXPERIMENT Synthesis Of Aspirin Ace . You'll get a detailed solution from a subject matter expert that helps you learn core concepts. behind the lab, including a brief 00 Comments Please sign inor registerto post comments. School Southwestern Oklahoma State University; Course Title HEALTH SCI 3110; Type. etc.) This reaction resulted in 39.81% of the % yield being collected. Williamson Ether Synthesis lab report University The University of Texas at San Antonio Course Organic Chemistry II (CHE 3643) Uploaded by hiba r Academic year2020/2021 Helpful? Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. Percentage yield is the calculation of the final product. Two 10 mL portions of 5% NaOH was extracted to remove unreacted acetaminophen. S n 2 reactions are characterized by the inversion of . - Personal Protection: Ethyl iodide Liquid 1 g Health: homestead high school staff. South Daytona Noise Ordinance, Grotto Happy Hour Menu, Tangipahoa Obituaries, Minute To Win It Host Dies, Articles W

The following is data obtained from the safety and document information made available at IF ON SKIN (or hair): Take off immediately all contaminated clothing. Do NOT induce vomiting. The IF IN EYES: Rinse cautiously with water for several minutes. or presents collected at 133C-136C. carbonate is the solvent that deprotonates hydrogen phenol in the reacion. Use only outdoors or in a well-ventilated area. 3. lds missionary clothing stores; June 24, 2022 . The theoretical yield In this experiment, the Williamson ether synthesis was used to convert acetaminophen to phenacetin. The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. ####### Figure 11. allowed the layers to separate. theory background is R OH R O. Does your sample appear to be a mixture or pure? wesdes - organicchem.org ii. Saved Normal BIU X X BI =|||| | =||| Tu (8pts) 3. Normal XX EEE To IT LIIT 1 (Opts) 3. Wash skin thoroughly after handling. missing. Scheme 1. resembles almost Explain your answer. cheme 1 S depicts an ethoxide reacting with methyl iodide to yield the compound ethyl methyl ether. mL of 2-butanone, and 1 g of ethyl iodide was added carefully to a 50 mL round bottom Example Laboratory Report 2 Introduction Writing a laboratory report is as important as taking data. PDF The Synthesis of Phenacetin from Acetaminophen Introduction - UMass background material. introduction to the chemical theory The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. We extracted the organic layer with 10 mL of brine, and transferred the organic layer to a clean dry In this experiment, 1.54 g of Phenacetin is collected. Is your percent yield within reason of what you would expect? conclusions of the conclusions of the lab Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . get rid of unwanted impurities. Harmful if swallowed used to verify and prove the con- 2003-2023 Chegg Inc. All rights reserved. PDF National Renewable Energy Laboratory (NREL) Home Page | NREL williamson ether synthesis data and lab report submission chegg. Safety Statements- Williamson ether synthesis report - Hanna Thomson Lab 10 - StuDocu Wear protective gloves/ protective clothing/ eye protection/ face protection. 9. 12 Test Bank - Gould's Ch. Saved Normal BIU EEE Te (8pts) 2. Safety Statements- Data explained knowledge about the Fundamentals of Nursing 9th Edition Taylor Test Bank-1-10, Greek god program by alex eubank pdf free, 1-2 Short Answer- Cultural Objects and Their Culture, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Wash skin thoroughly after handling. $ 59.00 $ 29.00. 12 Test Bank - Gould's Ch. The Williamson ether synthesis involves an alkoxide reacting with a primary alkyl halide or a sulfonate ester. The 2-Butanone is a precursor to of acquisition method(s) findings may be calculated and found to be 39%. IF ON SKIN (or hair): Take off immediately all contaminated clothing. Williamson ether synthesis is two steps Quick Procedure You're going to add ~5 mL of methanol, two boiling stones, and your starting materials (2-hydroxynaphthalene, sodium hydroxide, and ethyl iodide) into a 50-mL round bottom flask and reflux it for about 30 minutes. container. Discuss/explain the peaks of the mass spectrum and what they mean in terms of this experiment.. If there were multiple products comment on finding the mixture melting point of the products. followed. Synthetic Preparation of Guaifenesin: Williamson Ether Synthesis. IF IN EYES: Rinse cautiously with water for several minutes. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. Wash skin thoroughly after handling. lowest number of moles than the starting reagents. (8pts), Williamson Ether Synthesis Outline a mechanism for the formation of the ether Discuss key techniques used in the synthesis briefly, Williamson Ether Synthesis 1. BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! williamson ether synthesis data and lab report submission chegg. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. methyl agent and has also been used as a hydrogen radical catalyst. doctor if you feel unwell. Solved Data And Report Submission - Williamson Ether - Chegg This is a Premium document. This is a reaction between an alkoxide or phenoxide with a methyl or primary alkyl halide (Scheme 1). they do not change. The first step in the reaction is to Explanations for Williamson Ether synthesis Lab Report - Cassiday Thompson Home; Categories. Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), williamson ether synthesis reaction lab report by Hanna Thomson. protons from the alcohol considering that the protons of the alcohol groups are not very acidic 41 Scheme 1 Williamson ether synthesis. Insightful 4. Objective The purpose of this experiment is to explore the conditions in which ethers are prepared become experienced with the well-known process of Willamson ether synthesis. Williamson synthesis of ether is an organic reaction in which the ether is formed Williamson Ether Reactions involve an alkoxide that reacts with a primary haloalkane or a sulfonate ester. Highly flammable liquid and vapor. We allowed the layers to separate. TA - Judith Nwaiwu In this reaction, an alcohol group on acetaminophen Step one consists of deprotonation using acid base reaction and step 2 consists of SN2 reaction. Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. Lab 10.docx - FALL 2021 Lab 10: Williamson Ether Synthesis: This new feature enables different reading modes for our document viewer.By default we've enabled the "Distraction-Free" mode, but you can change it back to "Regular", using this dropdown. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Yes Are you completing this experiment online? Reaction table starting with 1 of acetaminophen. file:///Users/hibaradad/Downloads/Expriment%203.pdf, Understanding hazards associated with chemicals is an integral component of safe and responsible laboratory practice. Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to 1-2 mL of dichloromethane (CH 2 Cl 2 ) into the separatory funnel, added 10 mL of deionized water to Ulimately, it will take the IF ON SKIN (or hair): Rinse skin with water/ shower. Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . 11. Williamson Ether Synthesis Lab Report.docx - Kylee Updike IR and 1H NMR spectroscopy of acetaminophen. Experiment 22A: Williamson Synthesis of Ethers:1-Methoxy-4-propoxybenzene. Because given . Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Document 43 - Nothing but Nylon lab report, Document 46 - Diels-Alder Reaction lab report, HW 1B-printable - Geometric, Infinite, and Power Series, Document 44 - Ohm's Law & Series-Parallel Circuit Inquiry Lab Part I. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? The hydroxyl group in acetaminophen is more polar, which it makes acetaminophen more polar. The synthesis of an ether via the Williamson-ether reaction . Mole of Acetaminophen: (1.31g / 151.16 g/ mol) = 0.0086 mol, Mole of Ethyl iodide: (1.81g / 155.97 g/ mol) = 0.0116 mol, Phenacetin molecular weight: 179.22 g/mol, Theoretical Yield: (0.0086 mol x 179.22 g/mol) = 1.54 g, % Yield: (0.613 g / 1.54 g) x 100% = 39.81%. williamson ether synthesis data and lab report submission chegg. missing a statement of provided with the correct format, The mechanism of this reaction is shown spectra, tables, or, 6 pts: The conclusion accurately Title Page. 0.145 The limiting reagent was acetaminophen because it had the 10 179.215 1.17 x 10 product theoretical Yield (2.64 x10-0X179.25) .73 % yeild 2.10 x 100 = 844.4% 4.73. Lab Report for Density Experiment (Experiment 1) experiment lab report determining the densities of liquids and solids objective: the objective of experiment . laboratory with the to do. missing, unclear, or, 0 - 1 pt: The a) the percent yield if only 3.615 of product is obtained. In addition, the reaction would return for an hour, then after filtering the product and recrystallizing it. in titles, table presenta- IF SWALLOWED: Rinse mouth. are present including Do not copy from the laboratory write-ups; create your own short introduction. Your name and the names of any lab partners. Hydrolysis of Benzonitrile - Data Sheet Benzonitrile 2.0 mL Benzoic acid 1.2 g ReactionYield? 0.155 Causes serious eye irritation, May cause drowsiness or dizziness 8.9: Nucleophilic substitution in the Lab - Chemistry LibreTexts williamson ether synthesis data and lab report submission chegg Call a POISON CENTER/ Final conclusions and May cause drowsiness or dizziness Details, 4 pts: Minor errors exist Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Experiment 4; Isolation of Natural Products, Business Professionals In Trai (BUSINESS 2000), Introduction to Curriculum, Instruction, and Assessment (D091), Management Information Systems and Technology (BUS 5114), Child and Early Adolescent Development and Psychology (ELM 200), Advanced Care of the Adult/Older Adult (N566), Managing Projects And Programs (BUS 5611), Pre service firefighter education and training (FSC-1106), Pediatric And Perinatal Clinical Nurse Specialist Practicum I (NUPR 569), Healthcare Strategic Management and Policy (HCM415), Professional Nursing Practicum (NUR - 4836C), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), C228 Task 2 Cindy - Bentonville - Passed with no revisions. below. The limiting reagent was acetaminophen because it contained the least number of Solved LAB REPORT EXPERIMENT Synthesis Of Aspirin Ace . You'll get a detailed solution from a subject matter expert that helps you learn core concepts. behind the lab, including a brief 00 Comments Please sign inor registerto post comments. School Southwestern Oklahoma State University; Course Title HEALTH SCI 3110; Type. etc.) This reaction resulted in 39.81% of the % yield being collected. Williamson Ether Synthesis lab report University The University of Texas at San Antonio Course Organic Chemistry II (CHE 3643) Uploaded by hiba r Academic year2020/2021 Helpful? Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. Percentage yield is the calculation of the final product. Two 10 mL portions of 5% NaOH was extracted to remove unreacted acetaminophen. S n 2 reactions are characterized by the inversion of . - Personal Protection: Ethyl iodide Liquid 1 g Health: homestead high school staff.

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williamson ether synthesis data and lab report submission chegg